ANR Analytical Lab 

835

835 SOLUBLE ELEMENTS

Solubles: Al, B, Ca, Cu, Fe, K, Mg, Mn, Na, Si, Zn
Quantitative determination by AAS, AES and ICP-AES.

Summary: This method quantitatively determines the concentration of the listed elements in water samples by flame Atomic Absorption and Emission Spectrometry (AAS, AES) and Inductively Coupled Plasma Atomic Emission Spectrometry (ICP-AES). Approximately 100 mL per sample is requested. If sample is limited, some analyses are done simultaneously so the total sample required may be reduced. The EPA recommends that water for soluble analytes be filtered and acidified at the time of collection. Lower detection limits than those listed in the table below may be possible. Contact the lab if lower detection limits are needed or if elements not listed in the table are needed.

Element MDL (mg/L) Instrument(s)
Ag 0.01 ICP
Al 0.05 ICP
B 0.1 ICP
Ca 0.5 ICP
Cd 0.005 ICP
Cr 0.005 ICP
Cu 0.1 ICP or AAS
Fe 0.1 ICP or AAS
K 0.05 AES
Mg 0.5 ICP
Mn 0.1 ICP or AAS
Mo 0.01 ICP
Na 0.1 AES
Ni 0.05 ICP
P 0.05 ICP
Pb 0.05 ICP
Si 0.1 ICP
Zn 0.02 ICP or AAS

EPA Method 200.7, Trace Elements in Water Solids, and Biosolids by Inductively Coupled Plasma-Atomic Emission Spectrometry

EPA Method 258.1, Potassium (AA, Direct Aspiration)

EPA Method 273.1, Sodium (AA, Direct Aspiration)